低温强磁场拉曼与光电测试系统-西湖大学物质科学公共实验平台

生产厂家	Horiba+Attocube	型号	HORIBA LabRam Odyssey and Attocube attoDRY2100
制造国家	美国、法国	分类号
放置地点	云谷校区E10-B109（学术环地下一层）	出厂日期	2024/06/01
购置日期	2022/10/24	入网时间	2024/09/12
主要规格及技术指标	拉曼主机特性： 1. 最低拉曼分辨率：≤0.65 cm-1（585 nm氖灯线半高宽、1800刻线光栅） 2. 光谱检测范围：200-1550 nm（液氮降温CCD及InGaAs探测器） 3. 提供5路激光器：266、325、532、785及1064 nm及相应Edge与PL滤光片 4. 提供5组闪耀光栅：100、300、600、1800及2400线/mm 室温环境： 1. 提供75×50 mm大行程XYZ平台（50 nm步进）和SWIFT/DuoScan成像模块 2. 提供多颗物镜：5x、10x、50x、100x消色差物镜，15x、40x、74x紫外物镜，50x近红外物镜低温环境： 1. 提供1.8-300 K宽温区低温环境，温度波动小于0.01 K 2. 提供9+3 T矢量Z-X轴磁场环境，磁场均匀度≤0.1%（Z轴） 3. 提供专用低温强场消色差物镜（NA 0.8、520-695与700-985nm波段） 4. 提供三自由度位移器（5×5×4.8 mm行程）及扫描器（30×30×30 μm行程） Raman System Features: · Minimum Raman resolution: ≤0.65 cm⁻¹ (585 nm neon lamp line FWHM, 1800-groove/mm grating). · Spectral detection range: 200–1550 nm (liquid-nitrogen-cooled CCD and InGaAs detectors). · Equipped with 5 excitation lasers: 266, 325, 532, 785, and 1064 nm, along with corresponding Edge and PL filters. · Five blazed gratings: 100, 300, 600, 1800, and 2400 lines/mm. Ambient Temperature Capabilities: · Large-range XYZ stage (75 × 50 mm, 50 nm step resolution) integrated with SWIFT/DuoScan imaging modules. · Multiple objectives: 5×, 10×, 50×, 100× achromatic objectives; 15×, 40×, 74× UV objectives; 50× near-infrared objective. Cryogenic Capabilities: · Temperature range: 1.8–300 K with temperature stability < 0.01 K. · 9+3 T vector Z-X axis magnetic field environment, magnetic field uniformity ≤0.1% (Z-axis). · Specialized cryogenic achromatic objectives (NA 0.8, 520–695 nm and 700–985 nm bands). · Three-axis displacement system (5 × 5 × 4.8 mm travel range) and scanner (30 × 30 × 30 μm travel range).
主要功能及特色	本系统为集成化高性能拉曼光谱分析平台，结合Horiba Odyssey光谱仪与Attocube attoDRY2100低温恒温器，具备紫外-可见-近红外全波段检测能力。光谱仪配备液氮冷却CCD（200-1050 nm）、InGaAs探测器（800-1550 nm），以及五组闪耀光栅（100、300、600、1800及2400线/mm），最高实现低至0.35 cm⁻¹的超高分辨率。光谱仪具备机械针孔共焦系统（10-1000 μm可调）及双消色差共焦光路（UV/VIS），支持四种数据采集模式，可满足单窗口、多窗口及连续扫描需求。系统集成五波长激光器（266、325、532、785及1064 nm）及相应Edge与PL滤光片，配合75×50 mm大行程XYZ平台（50 nm步进）和SWIFT/DuoScan成像模块，可完成kHz级超快扫描与二维拉曼成像。低温模块attoDRY2100基于脉冲管制冷技术，提供1.8-300 K宽温区与9+3 T矢量Z-X轴磁场环境，样品腔体直径≥49 mm，磁场均匀度≤0.1%（Z轴）。配备专用消色差低温物镜（NA 0.8、520-695与700-985nm波段）、三自由度位移器（5×5×4.8 mm行程）及扫描器（30×30×30 μm行程），支持SHG测量与低温电学测试。本系统集成偏振分析、光电流联用功能，通过Labspec 6与LabVIEW软件实现自动化控制，可广泛应用于二维材料、半导体、新能源等领域，支持莫尔超晶格、量子点、自旋极化子等前沿研究的多维表征。 This system is an integrated high-performance Raman spectroscopy platform combining the Horiba Odyssey spectrometer with the Attocube attoDRY2100 cryostat, offering full-spectrum detection capabilities from ultraviolet to visible and near-infrared ranges. The spectrometer features a liquid-nitrogen-cooled CCD (200–1050 nm), an InGaAs detector (800–1550 nm), and five blazed gratings (100, 300, 600, 1800, and 2400 lines/mm), achieving an ultra-high resolution as low as 0.35 cm⁻¹. Equipped with a mechanical pinhole confocal system (adjustable from 10 to 1000 μm) and dual achromatic confocal optical paths (UV/VIS), it supports four data acquisition modes to meet single-window, multi-window, and continuous scanning requirements. The system integrates five excitation lasers (266, 325, 532, 785, and 1064 nm) with corresponding Edge and PL filters, combined with a large-range XYZ stage (75 × 50 mm, 50 nm step resolution) and SWIFT/DuoScan imaging modules, enabling kHz-level ultrafast scanning and 2D Raman imaging. The attoDRY2100 cryogenic module, based on pulse-tube refrigeration technology, provides a wide temperature range of 1.8–300 K and a 9+3 T vector Z-X axis magnetic field environment. The sample chamber has a diameter ≥49 mm, with magnetic field uniformity ≤0.1% (Z-axis). It includes specialized achromatic cryogenic objectives (NA 0.8, 520–695 nm and 700–985 nm bands), a three-axis displacement system (5 × 5 × 4.8 mm travel), and a scanner (30 × 30 × 30 μm travel), supporting SHG measurements and low-temperature electrical testing. Integrated with polarization analysis and photocurrent coupling functions, the system enables automated control via Labspec 6 and LabVIEW software. It is widely applicable to 2D materials, semiconductors, and new energy research, supporting multidimensional characterization for cutting-edge studies on Moire superlattices, quantum dots, and spin polaritons.
主要附件及配置	测试系统可与室温环境石英视窗的探针冷热台组合使用，可覆盖-195至400 ℃温度范围，真空度＜1 Pa，兼容电学探针（4组BNC/SMA接口）。 The testing system can be integrated with a thermal probe station equipped with quartz viewports for ambient temperature environments, covering a temperature range from -195 °C to 400 °C, with a vacuum pressure below 1 Pa, and compatible with electrical probes featuring four BNC/SMA connectors.
开放预约
计费信息	校内自主上机：260元/小时；培训400元/小时委托测试：校内390元/小时；校外650元/小时 Interanl charge: Independent operation 260CNY/hour; Training 400CNY/hour.

准备中

类型	项目	细则	校内	校外	说明
自主上机	自主操作	需预约并经过培训和考核	260元/时	/	设备因人为因素造成的损失需课题组承担
委托测试	常规项目	预约前请与管理员充分沟通，以制定合适的测试方案	390元/时	650元/时	特殊、批量或复杂样品价格面议
培训	仪器培训	一对一/一对二培训	400元/时	/	参加培训前须认真研读自主学习SOP

仪器编号		联系方式	15222051973
放置地点	云谷校区E10-B109（学术环地下一层）	开放范围	自主测试：校内；送样测试：校内/校外
自主操作	https://share.westlake.edu.cn/lims/!equipments/equipment/index.1117.reserv	送样检测	https://share.westlake.edu.cn/lims/!equipments/equipment/index.1117.sample
实验室		职位
邮箱	hongsiyuan@westlake.edu.cn